Innovative synthetic chemist specializing in inorganic and organometallic synthesis, air-sensitive techniques, and reaction development. Expertise in glovebox and Schlenk line chemistry, analytical characterization, and troubleshooting complex reactions. Developed new synthetic methodologies and contributed to impactful publications through multidisciplinary collaboration.
Overview
10
10
years of professional experience
Work History
AI Training Specialist (Chemistry Domain Expert)
Freelance
09.2023 - Current
Annotated and validated thousands of chemical reaction datasets, enhancing quality of machine learning models
Applied domain knowledge in chemistry to ensure data consistency and accuracy, contributing to high-quality client prompts
Graduate Research Assistant
University of California, Irvine
09.2018 - 06.2023
Synthesized and characterized novel air-sensitive organometallic complexes leading to the discovery of a new ligand capable of stabilizing the low oxidation state of lanthanides and actinides
Collaborated with Los Alamos National Laboratory to design reaction conditions for uranium complexes, facilitating expansion to neptunium and plutonium.
Designed a new protocol to collect X-ray photoelectron spectra of highly reactive lanthanide complexes to explore the low oxidation state electron configuration
Established and optimized electrochemical instrumentation, enhancing group's analytical characterization capabilities.
Managed elemental analysis instrumentation, ensuring maintenance, calibration, troubleshooting, and user training for optimal laboratory performance.
Maintained detailed experimental records and analytical data to ensure reproducibility and support publication-quality research.
Graduate Teaching Assistant
University of California, Irvine
09.2018 - 06.2023
Trained 500+ students on laboratory instrumentation, data collection, safety procedures to enhance practical skills and ensure compliance
Troubleshot experimental and instrumentation issues in real time to maintain experiment integrity and minimize disruptions
Undergraduate Research Assistant
West Virginia University
01.2017 - 05.2018
Researched nickel-catalyzed cross-coupling reactions to elucidate intermediates
Assisted in reaction optimization and mechanistic studies
Education
Ph. D. - Chemistry
University of California, Irvine
Irvine, California
06-2023
B.S. - Chemistry, Minor in Biology
West Virginia University
Morgantown, West Virginia
05-2018
Skills
Inorganic and organic synthesis
Manipulation of air sensitive compounds using glovebox and Schlenk line techniques
Multinuclear and paramagnetic NMR spectroscopy
IR spectroscopy
UV-visible spectroscopy
Elemental analysis
X-ray crystallography
Mass spectrometry
X-ray photoelectron spectroscopy
GC-MS
DSC
TGA
MestReNova
TopSpin
CasaXPS
Olex2
SHELX
Publications
Huh, D. N., Ciccone, S. R., Bekoe, S., Roy, S., Ziller, J. W., Furche, F., Evans, W. J., Synthesis of LnII-in-Cryptand Complexes by Chemical Reduction of LnIII-in-Cryptand Precursors: Isolation of a NdII-in-Cryptand Complex., Angew. Chem. Int. Ed., 12/20, 59, 16141–16146
Huh, D. N., Bruce, J. P., Balasubramani, S. G., Ciccone, S. R., Furche, F., Hemminger, J. C., Evans, W. J., High-Resolution X-ray Photoelectron Spectroscopy of Organometallic (C5H4SiMe3)3LnIII and [(C5H4SiMe3)3LnII]1- Complexes (Ln = Sm, Eu, Gd, Tb)., J. Am. Chem. Soc., 10/21, 143, 16610-16620
Huh, D. N., Barlow, J. M., Ciccone, S. R., Ziller, J. W., Yang, J. Y., Evans, W. J., Stabilization of U(III) to Oxidation and Hydrolysis by Encapsulation using 2.2.2-Cryptand., Inorg. Chem., 12/20, 59, 17077-17083
Huh, D. N., Ciccone, S. R., Moore, W. N. G., Ziller, J. W., Evans, W. J., Synthesis of Ba(II) Analogs of Ln(II)-in-(2.2.2-Cryptand) and Layered Hexagonal Net Ln(II) Complexes, [(THF)Cs(µ-η5:η5-C5H4SiMe3)3LnII]n., Polyhedron, 12/21, 210, 115393
Goodwin, C. A. P., Ciccone, S. R., Bekoe, S., Majumdar, S., Scott, B. L., Ziller, J. W., Gaunt, A. J., Furche, F., Evans, W. J., 2.2.2-Cryptand Complexes of Neptunium(III) and Plutonium(III)., Chem. Comm., 02/22, 58, 997-700
Green, K., Honeycutt, A. P., Ciccone, S. R., Grice, K. A., Petersen, J. L., Hoover, J. M., A Redox Transmetalation Step in Nickel-Catalyzed C–C Coupling Reactions., ACS Catal., 09/23, 13, 6375–6381
Part time Chemistry Tutor and Laboratory Demonstrator at The University Of ZambiaPart time Chemistry Tutor and Laboratory Demonstrator at The University Of Zambia