Summary
Overview
Work History
Education
Skills
Publications
Timeline
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Sierra Ciccone

Youngstown,OH

Summary

Innovative synthetic chemist specializing in inorganic and organometallic synthesis, air-sensitive techniques, and reaction development. Expertise in glovebox and Schlenk line chemistry, analytical characterization, and troubleshooting complex reactions. Developed new synthetic methodologies and contributed to impactful publications through multidisciplinary collaboration.

Overview

10
10
years of professional experience

Work History

AI Training Specialist (Chemistry Domain Expert)

Freelance
09.2023 - Current
  • Annotated and validated thousands of chemical reaction datasets, enhancing quality of machine learning models
  • Applied domain knowledge in chemistry to ensure data consistency and accuracy, contributing to high-quality client prompts

Graduate Research Assistant

University of California, Irvine
09.2018 - 06.2023
  • Synthesized and characterized novel air-sensitive organometallic complexes leading to the discovery of a new ligand capable of stabilizing the low oxidation state of lanthanides and actinides
  • Collaborated with Los Alamos National Laboratory to design reaction conditions for uranium complexes, facilitating expansion to neptunium and plutonium.
  • Designed a new protocol to collect X-ray photoelectron spectra of highly reactive lanthanide complexes to explore the low oxidation state electron configuration
  • Established and optimized electrochemical instrumentation, enhancing group's analytical characterization capabilities.
  • Managed elemental analysis instrumentation, ensuring maintenance, calibration, troubleshooting, and user training for optimal laboratory performance.
  • Maintained detailed experimental records and analytical data to ensure reproducibility and support publication-quality research.

Graduate Teaching Assistant

University of California, Irvine
09.2018 - 06.2023
  • Trained 500+ students on laboratory instrumentation, data collection, safety procedures to enhance practical skills and ensure compliance
  • Troubleshot experimental and instrumentation issues in real time to maintain experiment integrity and minimize disruptions

Undergraduate Research Assistant

West Virginia University
01.2017 - 05.2018
  • Researched nickel-catalyzed cross-coupling reactions to elucidate intermediates
  • Assisted in reaction optimization and mechanistic studies

Education

Ph. D. - Chemistry

University of California, Irvine
Irvine, California
06-2023

B.S. - Chemistry, Minor in Biology

West Virginia University
Morgantown, West Virginia
05-2018

Skills

  • Inorganic and organic synthesis
  • Manipulation of air sensitive compounds using glovebox and Schlenk line techniques
  • Multinuclear and paramagnetic NMR spectroscopy
  • IR spectroscopy
  • UV-visible spectroscopy
  • Elemental analysis
  • X-ray crystallography
  • Mass spectrometry
  • X-ray photoelectron spectroscopy
  • GC-MS
  • DSC
  • TGA
  • MestReNova
  • TopSpin
  • CasaXPS
  • Olex2
  • SHELX

Publications

  • Huh, D. N., Ciccone, S. R., Bekoe, S., Roy, S., Ziller, J. W., Furche, F., Evans, W. J., Synthesis of LnII-in-Cryptand Complexes by Chemical Reduction of LnIII-in-Cryptand Precursors: Isolation of a NdII-in-Cryptand Complex., Angew. Chem. Int. Ed., 12/20, 59, 16141–16146
  • Huh, D. N., Bruce, J. P., Balasubramani, S. G., Ciccone, S. R., Furche, F., Hemminger, J. C., Evans, W. J., High-Resolution X-ray Photoelectron Spectroscopy of Organometallic (C5H4SiMe3)3LnIII and [(C5H4SiMe3)3LnII]1- Complexes (Ln = Sm, Eu, Gd, Tb)., J. Am. Chem. Soc., 10/21, 143, 16610-16620
  • Huh, D. N., Barlow, J. M., Ciccone, S. R., Ziller, J. W., Yang, J. Y., Evans, W. J., Stabilization of U(III) to Oxidation and Hydrolysis by Encapsulation using 2.2.2-Cryptand., Inorg. Chem., 12/20, 59, 17077-17083
  • Huh, D. N., Ciccone, S. R., Moore, W. N. G., Ziller, J. W., Evans, W. J., Synthesis of Ba(II) Analogs of Ln(II)-in-(2.2.2-Cryptand) and Layered Hexagonal Net Ln(II) Complexes, [(THF)Cs(µ-η5:η5-C5H4SiMe3)3LnII]n., Polyhedron, 12/21, 210, 115393
  • Goodwin, C. A. P., Ciccone, S. R., Bekoe, S., Majumdar, S., Scott, B. L., Ziller, J. W., Gaunt, A. J., Furche, F., Evans, W. J., 2.2.2-Cryptand Complexes of Neptunium(III) and Plutonium(III)., Chem. Comm., 02/22, 58, 997-700
  • Green, K., Honeycutt, A. P., Ciccone, S. R., Grice, K. A., Petersen, J. L., Hoover, J. M., A Redox Transmetalation Step in Nickel-Catalyzed C–C Coupling Reactions., ACS Catal., 09/23, 13, 6375–6381

Timeline

AI Training Specialist (Chemistry Domain Expert)

Freelance
09.2023 - Current

Graduate Research Assistant

University of California, Irvine
09.2018 - 06.2023

Graduate Teaching Assistant

University of California, Irvine
09.2018 - 06.2023

Undergraduate Research Assistant

West Virginia University
01.2017 - 05.2018

Ph. D. - Chemistry

University of California, Irvine

B.S. - Chemistry, Minor in Biology

West Virginia University
Sierra Ciccone